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1 article(s) from Demirtas, İlknur

Bis(vinylenedithio)tetrathiafulvalene analogues of BEDT-TTF

Erdal Ertas,
İlknur Demirtas and
Turan Ozturk

Beilstein J. Org. Chem. 2015, 11, 403–415, doi:10.3762/bjoc.11.46

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Graphical Abstract

Figure 1: Chemical structure of the TTF analogues and TCNQ.

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Figure 2: Oxidation states of TTF.

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Figure 3: 1,4-Dithiin and thiophene fused TTF analogues from 1,8-diketone.

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Scheme 1: Reaction mechanism of fused 1,4-dithiin and thiophene ring systems.

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Scheme 2: Reaction conditions (i) LR, toluene, reflux, overnight; (ii) P₄S₁₀, toluene, reflux, 3 h.

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Scheme 3: Proposed mechanism for side products.

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Scheme 4: Reaction conditions (i) Hg(OAc)₂, AcOH/CHCl₃, rt, 1h; (ii) (EtO)₃P, N₂, 3 h, 110 °C.

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Scheme 5: Reaction conditions (i) iPr₂NEt, MEMCl, THF, rt, 12 h; (ii) LiAlH_4, dry ether, rt, 24 h; (iii) tosy...

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Scheme 6: Reagents and conditions (i) P₄S₁₀, toluene, reflux, dark, 3 h; (ii) P₄S₁₀, toluene, reflux, 3 h; (i...

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Scheme 7: Reagents and conditions (i) Hg(OAc)₂–AcOH, CHCl₃, 3 h, rt; (ii) (EtO)₃P, 110 °C, N₂, 2 h.

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Scheme 8: Charge transfer complex of 5,5',6,6'-tetraphenyl-2,2'-bi([1,3]dithiolo[4,5-b][1,4]dithiinylidene) 52...

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Scheme 9: Reaction conditions (i) (EtO)₃P, 110 °C, N₂, 2 h.

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Scheme 10: Reaction conditions (i) EtOH, reflux, overnight; (ii) diisopropylethylamine in CH₂Cl₂, room tempera...

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Scheme 11: Reaction and conditions (i) P₄S₁₀, NaHCO₃, toluene, reflux, 3 h; (ii) P₄S₁₀, p-TSA, toluene, reflux...

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Review

Published 27 Mar 2015

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